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Publication details

Document type
Journal articles

Document subtype
Full paper

Title
X-ray characterization of an unusual product obtained from [VO(Sal–Phe)(H2O)] in H2O\\pyridine solutions

Participants in the publication
A. Bernalte (Author)
F.J.G. Barros (Author)
I. Cavaco (Author)
J.Costa Pessoa (Author)
R.D. Gillard (Author)
F.J. Higes (Author)
I. Tomaz (Author)
Dep. Química e Bioquímica
 CQE
Summary
A vanadium(V) dimer [\\VO2(py)(2)\\(2)(mu-C2O4)] 1, has been isolated from a solution of [VO(sal-Phe)(H2O)] 2 (sal-Phe = N-salicylidene-L-phenylalaninate) in H2O/pyridine. Its crystal and molecular structure has been determined by X-ray diffraction analysis, the oxalate acting as a symmetrical bis(chelating) bridge. Possible mechanisms for the formation of oxalate are briefly discussed.

Date of Publication
1998-09

Where published
Polyhedron

Publication Identifiers
ISSN - 0277-5387

Publisher
Elsevier BV

Volume
17
Number
19

Number of pages
6
Starting page
3269
Last page
3274

Document Identifiers
DOI - https://doi.org/10.1016/s0277-5387(98)00105-3
URL - http://dx.doi.org/10.1016/s0277-5387(98)00105-3

Rankings
SCOPUS Q1 (2019) - 3.9 - Materials Chemistry


Export

APA
A. Bernalte, F.J.G. Barros, I. Cavaco, J.Costa Pessoa, R.D. Gillard, F.J. Higes, I. Tomaz, (1998). X-ray characterization of an unusual product obtained from [VO(Sal–Phe)(H2O)] in H2O\\pyridine solutions. Polyhedron, 17, 3269-3274. ISSN 0277-5387. eISSN . http://dx.doi.org/10.1016/s0277-5387(98)00105-3

IEEE
A. Bernalte, F.J.G. Barros, I. Cavaco, J.Costa Pessoa, R.D. Gillard, F.J. Higes, I. Tomaz, "X-ray characterization of an unusual product obtained from [VO(Sal–Phe)(H2O)] in H2O\\pyridine solutions" in Polyhedron, vol. 17, pp. 3269-3274, 1998. 10.1016/s0277-5387(98)00105-3

BIBTEX
@article{52610, author = {A. Bernalte and F.J.G. Barros and I. Cavaco and J.Costa Pessoa and R.D. Gillard and F.J. Higes and I. Tomaz}, title = {X-ray characterization of an unusual product obtained from [VO(Sal–Phe)(H2O)] in H2O\\pyridine solutions}, journal = {Polyhedron}, year = 1998, pages = {3269-3274}, volume = 17 }